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Fig. 4. Non-steady-state diffusive flux estimator goodness-of-fit ( ${chi}$ ²) to simulated headspace concentrations (closed symbols) and flux (f₀) estimation accuracy (open symbols) in response to an instantaneous pressure perturbation ( ${Delta}$ P) induced at t = 0 min (positive perturbation) or at t = 10 min (negative perturbation). Data represent an experimental time constant ${tau}$ = 610 min. The solid lines are not fits, but connect the data points to aid the eye.