SSSAJ Journal of Natural Resources and Life Sciences Education
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Published in Soil Sci Soc Am J 34:351-353 (1970)
© 1970 Soil Science Society of America
677 S. Segoe Rd., Madison, WI 53711 USA
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Separation of Clay Minerals and Soil Clays Using Isopycnic Zonal Centrifugation1

C. W. Francis, Tsuneo Tamura, W. P. Bonner and J. W. Amburgey, Jr.2

ABSTRACT

The technique of isopycnic-zonal centrifugation in a continuous nonaqueous density gradient was used in the purification and separation of standard clay minerals and soil clays. A suspending agent (polyvinylpyrrolidone) compatible with tetrabromoethane and ethanol stabilized clay suspensions produced multiple banding of systems which otherwise flocculated into one band. Data from x-ray diffraction analyses revealed the technique is useful in purification of clay minerals and identification of clay minerals in soil clays; however the banding obtained from the clay fraction of a Dodge silt loam did not represent discrete bands of specific clay minerals.


NOTES

1 Research sponsored by the US Atomic Energy Commission under contract with the Union Carbide Corporation.

2 Scientists, Oak Ridge National Laboratory, and Development Engineer, Oak Ridge Gaseous Diffusion Plant, respectively.







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