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Published in Soil Sci Soc Am J 33:326-328 (1969)
© 1969 Soil Science Society of America
677 S. Segoe Rd., Madison, WI 53711 USA
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Fractionation of Phosphorus in Lake Sediments: Analytical Evaluation1

C. R. Frink2

ABSTRACT

Methods for the fractionation of P in soils were evaluated in the fractionation of P in lake sediments. Both Al-P and Fe-P may be determined readily and precisely by the Chang and Jackson procedure. Reductant-soluble P was more difficult: modifications of a citrate oxidation procedure utilizing KMnO4 produced an acceptable method. Large amounts of Fe in the Ca-P extracts caused low results, but this was overcome by limiting the aliquot size. Organic P determined by difference between total and inorganic P was not related to the organic matter content of the sediments. An alternative measure of inorganic P, obtained by summing the inorganic P fractions, yielded values for organic P which were correlated with organic matter.


NOTES

1 Contribution from The Connecticut Agr. Exp. Sta., New Haven.

2 Soil Chemist.

Received for publication August 29, 1968. Accepted for publication January 16, 1969.







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Copyright © 1969 by the Soil Science Society of America.