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ABSTRACT
A procedure is described which reduces the possibility of chemical alteration of soil organic matter during extraction, and which permits recovery of most of the solubilized organic matter as an acid-insoluble material low in ash. The essential features of the method are: (i) destruction of hydrated silicate minerals by pretreatment of the soil with 0.3N HF, (ii) recovery of organic matter by extraction first with 0.02M Na4P2O7 and then with 0.03N NaOH, and (iii) removal of inorganic contaminants by dialysis against 0.3N HF.
1 Contribution from the Department of Agronomy, University of Illinois, Urbana.
2 Former Research Assistant and Professor, respectively. The senior author is now Research Assistant, Michigan State University, East Lansing.
Received for publication June 16, 1967. Accepted for publication September 19, 1967.
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